7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

Base Information

Chemical Name:7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride
CAS No.:1434044-44-6
Molecular Formula:C₁₇H₁₆N₄
Molecular Weight:276.341
Hs Code.:

Synonyms:7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

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Chemical Property of 7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

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Technology Process of 7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

There total 10 articles about 7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1433992-85-8
tert-butyl 7-benzyl-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine-6(7H)-carboxylate

: 1434044-44-6
7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 2h;

Reference yield:

: 1433992-82-5
tert-butyl 3-benzyl-2-oxo-2,3-dihydro-1H-pyrido[2,3-e][1,4]diazepine-4(5H)-carboxylate

: 1434044-44-6
7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: Lawessons reagent / toluene / 3 h / 90 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

3: 1 h / 90 °C / Sealed tube; Microwave irradiation

4: toluene-4-sulfonic acid / toluene / 1 h / Reflux

5: hydrogenchloride / methanol / 2 h / 20 °C

With Lawessons reagent; hydrogenchloride; potassium carbonate; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: methyl 2-((2-(tert-butoxycarbonylamino)pyridin-3-yl)methylamino)-3-phenylpropanoate

: 1434044-44-6
7-benzyl-6,7-dihydro-5H-imidazo[1,2-a]pyrido[3,2-f][1,4]diazepine hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / methanol / 2 h / 20 °C

2: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3: dichloromethane; acetonitrile / Reflux

4: Lawessons reagent / toluene / 3 h / 90 °C

5: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

6: 1 h / 90 °C / Sealed tube; Microwave irradiation

7: toluene-4-sulfonic acid / toluene / 1 h / Reflux

8: hydrogenchloride / methanol / 2 h / 20 °C

With Lawessons reagent; hydrogenchloride; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;