Technology Process of C11H23NO3Si
There total 1 articles about C11H23NO3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1.1: pyridinium p-toluenesulfonate / benzene / 10 h / Reflux
2.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 4 h / -78 °C
2.2: 2 h
3.1: toluene-4-sulfonic acid / methanol; water / 4 h / 20 °C
4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 10 h / Inert atmosphere; Reflux
With
N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; methanol; water; ethyl acetate; benzene;
DOI:10.1002/ejoc.201100601
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / benzene / Reflux
2: trifluoroacetic acid / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
3: potassium carbonate / acetonitrile / 0 °C / pH 10 / Reflux
4: potassium carbonate / acetonitrile / 10 h / Reflux
5: palladium diacetate; potassium carbonate; triphenylphosphine / acetonitrile / 12 h / Inert atmosphere; Reflux
With
palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; trifluoroacetic acid;
In
dichloromethane; acetonitrile; benzene;
5: Heck coupling reaction;
DOI:10.1002/ejoc.201100601
