3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

Base Information

• Chemical Name: 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester
• CAS No.: 908865-26-9
• Molecular Formula: C₂₈H₃₁N₅O₃
• Molecular Weight: 485.586

Synonyms:3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

Chemical Property of 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

Chemical Property:

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Technology Process of 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

There total 2 articles about 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester (908865-25-8) → 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester (908865-26-9)

Guidance literature:

With copper (I) trifluoromethane sulfonate benzene; In N,N-dimethyl-formamide; toluene; at 130 ℃; for 0.216667h; microwave irradiation;

DOI:10.1016/j.ejmech.2006.03.008

Reference yield:

3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]prop-2-enyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester → 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester (908865-26-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 1 h / 20 °C / atmospheric pressure

2: 180 mg / copper(I) trifluoromethanesulfonate benzene complex / toluene; dimethylformamide / 0.22 h / 130 °C / microwave irradiation

With copper (I) trifluoromethane sulfonate benzene; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;

DOI:10.1016/j.ejmech.2006.03.008

Reference yield: 54.0%

3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester (908865-26-9) → 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; methanol; water; at 100 ℃; for 0.0333333h; microwave irradiation;

DOI:10.1016/j.ejmech.2006.03.008

upstream raw materials:

3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

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