3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

Base Information

Chemical Name:3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester
CAS No.:908865-25-8
Molecular Formula:C₃₃H₃₉N₅O₅
Molecular Weight:585.703
Hs Code.:

Synonyms:3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

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Chemical Property of 3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

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Technology Process of 3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

There total 1 articles about 3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]prop-2-enyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

: 908865-25-8
3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 1h; atmospheric pressure;
DOI:10.1016/j.ejmech.2006.03.008

Reference yield:

: 908865-25-8
3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

: 908865-26-9
3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

Guidance literature:: With copper (I) trifluoromethane sulfonate benzene; In N,N-dimethyl-formamide; toluene; at 130 ℃; for 0.216667h; microwave irradiation;
DOI:10.1016/j.ejmech.2006.03.008

Reference yield:

: 908865-25-8
3-[1-[3-[8-tert-butoxycarbonyl(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)]propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid ethyl ester

: 3-[1-[3-(5,6,7,8-tetrahydro[1,8]naphthyridin-2-yl)propyl]-7-deazahypoxanthinh-9-yl]-3-phenylacrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 180 mg / copper(I) trifluoromethanesulfonate benzene complex / toluene; dimethylformamide / 0.22 h / 130 °C / microwave irradiation

2: 54 percent / LiOH*H₂O / tetrahydrofuran; methanol; H₂O / 0.03 h / 100 °C / microwave irradiation

With lithium hydroxide; copper (I) trifluoromethane sulfonate benzene; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2006.03.008