bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

Base Information

Chemical Name:bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)
CAS No.:760997-14-6
Molecular Formula:C₃₅H₂₅IrN₆
Molecular Weight:721.844
Hs Code.:

Synonyms:bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

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Chemical Property of bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

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Technology Process of bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

There total 5 articles about bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [iridium(III)(μ-chloro)(2-phenylpyridine)2]2

: 25433-29-8
3-(pyridine-2-yl)-5-phenyl-1,2,4-triazole

: 760997-14-6
bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

Guidance literature:: With sodium carbonate; In 2-ethoxy-ethanol; at 130 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.dyepig.2016.03.006

Reference yield:

: 100-70-9,1232006-36-8
2-Cyanopyridine

: 760997-14-6
bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate; hydrazine hydrate / ethanol / 12 h / Inert atmosphere; Cooling with ice

2.1: sodium carbonate / tetrahydrofuran; N,N-dimethyl acetamide / 0.25 h / 0 °C / Inert atmosphere

2.2: 15 h / Inert atmosphere

3.1: sodium carbonate / 2-ethoxy-ethanol / 20 h / 130 °C / Inert atmosphere

With sodium carbonate; hydrazine hydrate; In tetrahydrofuran; 2-ethoxy-ethanol; ethanol; N,N-dimethyl acetamide;
DOI:10.1016/j.dyepig.2016.03.006

Reference yield:

: 1005-02-3
picolinamidrazone

: 760997-14-6
bis(2-phenylpyridine)[3-(2-pyridyl)-5-phenyl-1,2,4-triazole]iridium(III)

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / tetrahydrofuran; N,N-dimethyl acetamide / 0.25 h / 0 °C / Inert atmosphere

1.2: 15 h / Inert atmosphere

2.1: sodium carbonate / 2-ethoxy-ethanol / 20 h / 130 °C / Inert atmosphere

With sodium carbonate; In tetrahydrofuran; 2-ethoxy-ethanol; N,N-dimethyl acetamide;
DOI:10.1016/j.dyepig.2016.03.006