Technology Process of C27H37NO6
There total 15 articles about C27H37NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 25 ℃;
for 10h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 8.8 g / t-BuOK / tetrahydrofuran / 6 h / 20 °C
2.1: lithium borohydride / tetrahydrofuran / 0.5 h / 20 °C
2.2: tetrahydrofuran; methanol / 24 h / 20 °C
3.1: 3.9 g / NMO; TPAP / CH2Cl2 / 18 h / 20 °C
4.1: tetrahydrofuran / 11.5 h / -78 - 20 °C
4.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C
5.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C
6.1: NaBH4 / tetrahydrofuran; H2O / 0.5 h / 20 °C
7.1: 136 mg / triethylamine / CH2Cl2 / 10 h / 20 °C
With
hydrogenchloride; sodium tetrahydroborate; lithium borohydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; potassium tert-butylate; triethylamine;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol0706051
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrahydrofuran / 48 h / 20 °C
2.1: tetrahydrofuran / 11.5 h / -78 - 20 °C
2.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C
3.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C
4.1: NaBH4 / tetrahydrofuran; H2O / 0.5 h / 20 °C
5.1: 136 mg / triethylamine / CH2Cl2 / 10 h / 20 °C
With
hydrogenchloride; sodium tetrahydroborate; triethylamine;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol0706051
