2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

Base Information

Chemical Name:2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol
CAS No.:119204-08-9
Molecular Formula:C₂₅H₄₂O₄Si
Molecular Weight:434.692
Hs Code.:

Synonyms:2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

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Chemical Property of 2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

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Technology Process of 2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

There total 6 articles about 2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 119204-06-7
2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

: 119204-08-9
2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; for 0.5h; Ambient temperature;

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 119204-08-9
2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / ethyl(di-isopropyl)amine / CH₂Cl₂ / 4 h / Ambient temperature

2: 91 percent / toluene-p-sulphonic acid / 1 h / Ambient temperature

3: 1.) Mg powder / 1.) THF, reflux, 15 h; 2.) THF, -78 deg C, 3 h, then Rt

4: 97 percent / NaBH₄, cerium(III) chloride / methanol / 0.5 h / Ambient temperature

With sodium tetrahydroborate; cerium(III) chloride; toluene-4-sulfonic acid; magnesium; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

Reference yield:

: 58310-18-2
1,4-dihydro-2,6-dimethoxybenzoic acid

: 119204-08-9
2-Benzyloxymethoxymethyl-3-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Ambient temperature

2: 91 percent / ethyl(di-isopropyl)amine / CH₂Cl₂ / 4 h / Ambient temperature

3: 91 percent / toluene-p-sulphonic acid / 1 h / Ambient temperature

4: 1.) Mg powder / 1.) THF, reflux, 15 h; 2.) THF, -78 deg C, 3 h, then Rt

5: 97 percent / NaBH₄, cerium(III) chloride / methanol / 0.5 h / Ambient temperature

With sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; toluene-4-sulfonic acid; magnesium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;