(tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

Base Information

Chemical Name:(tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate
CAS No.:112506-19-1
Molecular Formula:C₆H₁₆LiN₂*C₁₈H₃₂B
Molecular Weight:382.411
Hs Code.:

Synonyms:(tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

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Technology Process of (tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

There total 1 articles about (tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: Li⁽¹⁺⁾*(C₆H₂(C₄H₉)3)BH₃^(1-) = Li(C₆H₂(C₄H₉)3)BH₃

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 112506-19-1
(tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

Guidance literature:: In hexane; stirring (1 h); filtn., concn. (vacuum), pptn. on cooling (-18°C), drying (vacuum); elem. anal.;

Reference yield: 53.0%

: 112506-19-1
(tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

: 112506-16-8
5,7-di-tert-butylhydroxy-3,3-dimethyl-1-boraindane

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

Guidance literature:: With hydrogenchloride; water; In diethyl ether; water; byproducts: H2, LiCl; addn. of HCl to ether soln. of borate (0°C), stirring (room temp., 1 h), aq. HCl addn.; drying of etheral phase (Na2SO4), solvent removal (vacuum), repptn. (pentane); elem. anal.;

Reference yield: 36.0%

: 112506-19-1
(tetramethylethylenediamine)lithium trihydro(2,4,6-tri-tert-butylphenyl)borate

: 112506-15-7
hydroxy(2,4,6-tri-tert-butylphenyl)borane

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

Guidance literature:: With water; In tert-butyl alcohol; byproducts: H2, LiOH; stirring (0°C, 6h, room temp., 12 h); solvent removal (vacuum), addn. of ether/water, drying of ether phase (Na2SO4), solvent removal (vacuum), recrystn. (pentane); elem. anal.;