[(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester
• CAS No.: 192310-93-3
• Molecular Formula: C₁₈H₂₄N₂O₄S
• Molecular Weight: 364.466

Synonyms:[(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

Chemical Property of [(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of [(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

There total 1 articles about [(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + 3-aminodihydrothiophen-2(3H)-one hydrochloride (6038-19-3) → [(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester (192310-93-3)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jm00052a002

Reference yield: 40.0%

[(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester (192310-93-3) → (tert-butoxycarbonyl)-L-phenylalanyl-D,L-homocysteine

Guidance literature:

With sodium hydroxide; In methanol; for 2h; Ambient temperature;

DOI:10.1021/jm00052a002

Reference yield:

[(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester (192310-93-3) → (S)-2-Amino-N-(2-oxo-tetrahydro-thiophen-3-yl)-3-phenyl-propionamide

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jm00052a002

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

3-aminodihydrothiophen-2(3H)-one hydrochloride

Downstream raw materials:

N-[(S)-1-(2-Oxo-tetrahydro-thiophen-3-ylcarbamoyl)-2-phenyl-ethyl]-isobutyramide

(S)-N-(2-Oxo-tetrahydro-thiophen-3-yl)-2-(2-phenoxy-acetylamino)-3-phenyl-propionamide

2-naphthoyl-L-phenylalanyl-D,L-homocysteine thiolactone

(S)-2-[3-(3,4-Dichloro-phenyl)-propionylamino]-N-(2-oxo-tetrahydro-thiophen-3-yl)-3-phenyl-propionamide

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