benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate

Base Information

Chemical Name:benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate
CAS No.:219700-73-9
Molecular Formula:C₄₄H₃₈O₈
Molecular Weight:694.781
Hs Code.:

Synonyms:benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate

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Technology Process of benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate

There total 2 articles about benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7141-98-2
2,4-bis-(benzyloxy)-6-methylbenzoic acid

: 219700-83-1
benzyl 4-benzyloxy-3,6-dihydroxy-2-methylbenzoate

: 219700-73-9
benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate

Guidance literature:: With trifluoroacetic anhydride; In toluene; for 12h;
DOI:10.1071/C98082

Reference yield:

: 214483-47-3
benzyl 4-benzyloxy-2-hydroxy-6-methylbenzoate

: 219700-73-9
benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-6-hydroxy-2-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 9.6 percent / 20 percent aq. sodium hydroxide, potassium persulfate / dioxane / 12 h / Ambient temperature

2: 90 percent / trifluoroacetic anhydride / toluene / 12 h

With sodium hydroxide; potassium peroxomonosulphate; trifluoroacetic anhydride; In 1,4-dioxane; toluene;
DOI:10.1071/C98082