1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

Base Information

Chemical Name:1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene
CAS No.:1554305-12-2
Molecular Formula:C₁₈H₁₈F₆O₂S
Molecular Weight:412.396
Hs Code.:

Synonyms:1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

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Technology Process of 1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

There total 2 articles about 1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1-ethynyl-4,4-dimethylcyclohexyl 3,5-bis(trifluoromethyl)benzenesulfinate

: 1554305-12-2
1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

Guidance literature:: With silver hexafluoroantimonate; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1002/adsc.201600986

Reference yield:

: 68483-62-5
1-ethynyl-4,4-dimethylcyclohexan-1-ol

: 39234-86-1
3,5-bis(trifluoromethyl)benzenesulfonyl chloride

: 1554305-12-2
1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; phosphonic acid diethyl ester / dichloromethane / 40 °C / Inert atmosphere

2: silver hexafluoroantimonate / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

With silver hexafluoroantimonate; triethylamine; phosphonic acid diethyl ester; In dichloromethane;
DOI:10.1002/adsc.201600986

Reference yield: 83.0%

: 1554305-12-2
1-((2-(4,4-dimethylcyclohexylidene)vinyl)sulfonyl)-3,5-bis(trifluoromethyl)benzene

: 1554305-49-5
(E)-1-((2-(4,4-dimethylcyclohex-1-en-1-yl)vinyl)sulfonyl)-3,5-bis-(trifluoromethyl)benzene

Guidance literature:: With palladium diacetate; tricyclohexylphosphine; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.6b00880