N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Base Information

Chemical Name:N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide
CAS No.:1453860-56-4
Molecular Formula:C₃₃H₄₈N₂O₃
Molecular Weight:520.756
Hs Code.:

Synonyms:N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Suppliers and Price of N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

There total 4 articles about N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1453860-48-4
N,N-dimethyl-3,12-dioxo-7-deoxycholic amide

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 1453860-56-4
N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Guidance literature:: With sodium acetate; In ethanol; at 70 ℃; for 3h;
DOI:10.3390/molecules18077436

Reference yield:

: 83-44-3
Deoxycholic acid

: 1453860-56-4
N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Guidance literature:: Multi-step reaction with 4 steps

1: Jones reagent / acetone / 0 °C

2: pyridine; oxalyl dichloride / toluene / 2 h / Cooling with ice

3: toluene / 0.17 h / 0 °C

4: sodium acetate / ethanol / 3 h / 70 °C

With pyridine; Jones reagent; oxalyl dichloride; sodium acetate; In ethanol; acetone; toluene;
DOI:10.3390/molecules18077436

Reference yield:

: 2958-05-6
3,12-dioxo-7-deoxycholic acid

: 1453860-56-4
N,N-dimethyl-3-O-benzyloximino-12-oxo-7-deoxycholic amide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; oxalyl dichloride / toluene / 2 h / Cooling with ice

2: toluene / 0.17 h / 0 °C

3: sodium acetate / ethanol / 3 h / 70 °C

With pyridine; oxalyl dichloride; sodium acetate; In ethanol; toluene;
DOI:10.3390/molecules18077436