1,1,1-trinitro-2-[(2,2,2-trinitroethoxy)methoxy]ethane

Base Information

• Chemical Name: 1,1,1-trinitro-2-[(2,2,2-trinitroethoxy)methoxy]ethane
• CAS No.: 6263-74-7
• Molecular Formula: C5H6 N6 O14
• Molecular Weight: 374.134
• Mol file: 6263-74-7.mol

Synonyms:Methane,bis(2,2,2-trinitroethoxy)- (7CI,8CI); Bis(2,2,2-trinitroethyl)formal;Bis(trinitroethoxy)methane; Trinitroethyl formal

Chemical Property of 1,1,1-trinitro-2-[(2,2,2-trinitroethoxy)methoxy]ethane

Chemical Property:

• Vapor Pressure: 5.28E-07mmHg at 25°C
• Boiling Point: 412.2°C at 760 mmHg
• Flash Point: 176.7°C
• Density: 1.865g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1,1-trinitro-2-[(2,2,2-trinitroethoxy)methoxy]ethane

There total 3 articles about 1,1,1-trinitro-2-[(2,2,2-trinitroethoxy)methoxy]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,2,2-trinitroethanol (918-54-7) + 1,7-diacetoxy-2,4,6-trinitro-2,4,6-triazaheptane (14173-62-7) → 1,1,1,7,7,7-hexanitro-3,5-dioxaheptane (6263-74-7)

Guidance literature:

With sulfuric acid; 14-15 deg C -> 20-22 deg C, 10 min, 20-22 deg C, 1 h;

DOI:10.1007/BF01435814

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,2,2-trinitroethanol (918-54-7) → 1,1,1,7,7,7-hexanitro-3,5-dioxaheptane (6263-74-7)

Guidance literature:

With sulfuric acid; In dichloromethane;

DOI:10.1021/jo01341a049

Reference yield:

→ 1,1,1,7,7,7-hexanitro-3,5-dioxaheptane (6263-74-7)

Guidance literature:

Trinitroethanol/konz. H2SO4, Paraformaldehyd;

upstream raw materials:

formaldehyd

2,2,2-trinitroethanol

1,7-diacetoxy-2,4,6-trinitro-2,4,6-triazaheptane

Downstream raw materials:

1,7-difluoro-1,1,7,7-tetranitro-3,5-dioxaheptane