2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

Base Information

Chemical Name:2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol
CAS No.:161032-73-1
Molecular Formula:C₂₆H₄₀N₂O₆
Molecular Weight:476.613
Hs Code.:

Synonyms:2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

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Chemical Property of 2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

Chemical Property:

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Technology Process of 2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

There total 3 articles about 2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161032-69-5
2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol

: 161032-73-1
2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; ethanol; for 4h; Ambient temperature;
DOI:10.1016/S0040-4039(00)74409-1

Reference yield:

: 90-02-8
salicylaldehyde

: 161032-73-1
2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / potassium carbonate / acetonitrile / 96 h / Heating

2: methanol; acetonitrile / 24 h / Heating

3: 1.) NaBH₄; 2.) aq. NaOH / tetrahydrofuran; ethanol / 4 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; potassium carbonate; In tetrahydrofuran; methanol; ethanol; acetonitrile;
DOI:10.1016/S0040-4039(00)74409-1

Reference yield:

: 161650-24-4
2-(2-(2-hydroxyethoxy)ethoxy)benzaldehyde

: 161032-73-1
2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; acetonitrile / 24 h / Heating

2: 1.) NaBH₄; 2.) aq. NaOH / tetrahydrofuran; ethanol / 4 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; methanol; ethanol; acetonitrile;
DOI:10.1016/S0040-4039(00)74409-1