2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol

Base Information

• Chemical Name: 2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol
• CAS No.: 161032-69-5
• Molecular Formula: C₂₆H₃₆N₂O₆
• Molecular Weight: 472.582
• Mol file: 161032-69-5.mol

Synonyms:

Chemical Property of 2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol

There total 2 articles about 2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

salicylaldehyde (90-02-8) → 2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol (161032-69-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / potassium carbonate / acetonitrile / 96 h / Heating

2: methanol; acetonitrile / 24 h / Heating

With potassium carbonate; In methanol; acetonitrile;

DOI:10.1016/S0040-4039(00)74409-1

Reference yield:

1,4-diaminobutane (110-60-1) + 2-(2-(2-hydroxyethoxy)ethoxy)benzaldehyde (161650-24-4) → 2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol (161032-69-5)

Guidance literature:

In methanol; acetonitrile; for 24h; Yield given; Heating;

DOI:10.1016/S0040-4039(00)74409-1

Reference yield:

2-(2-{2-[((E)-4-{[1-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-meth-(E)-ylidene]-amino}-butylimino)-methyl]-phenoxy}-ethoxy)-ethanol (161032-69-5) → 2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol (161032-73-1)

Guidance literature:

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; ethanol; for 4h; Ambient temperature;

DOI:10.1016/S0040-4039(00)74409-1

upstream raw materials:

1,4-diaminobutane

2-(2-(2-hydroxyethoxy)ethoxy)benzaldehyde

salicylaldehyde

Downstream raw materials:

2-(2-{2-[(4-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-benzylamino}-butylamino)-methyl]-phenoxy}-ethoxy)-ethanol

C₅₄H₆₄N₂O₁₄S₄