3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

Base Information

Chemical Name:3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one
CAS No.:1403230-67-0
Molecular Formula:C₃₄H₅₄N₂O₅Si₂
Molecular Weight:626.984
Hs Code.:

Synonyms:3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

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Chemical Property of 3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

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Technology Process of 3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

There total 1 articles about 3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: CF-1743

: 1403230-67-0
3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

Guidance literature:: With 1H-imidazole; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1002/cmdc.201200295

Reference yield:

: 1403230-67-0
3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

: C₃₂H₄₂N₄O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; methanol / 2 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With hydrogenchloride; methanol; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200295

Reference yield:

: 1403230-67-0
3-[3’,5’-di-O-(tert-butyldimethylsilyl)-2’-deoxy-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

: 1403230-69-2
3-[3’-O-(tert-butyldimethylsilyl)-2’-deoxy-5’-O-[2-(valylprolylamino)ethylcarbamoyl]-β-D-ribofuranosyl]-6-(p-pentylphenyl)-2,3-dihydrofuro[2,3-d]pyrimidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; methanol / 2 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

3: triethylamine / N,N-dimethyl-formamide / 24 h / 40 °C

With hydrogenchloride; methanol; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200295