N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

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Chemical Name:N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine
CAS No.:90072-45-0
Molecular Formula:C₁₂H₉N₇O₃S
Molecular Weight:331.315
Hs Code.:

Synonyms:N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

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Chemical Property of N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

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Technology Process of N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

There total 3 articles about N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 90072-41-6
4-Methyl-6-(4-nitro-benzylsulfanyl)-pyrimidine-2,5-diamine

: 90072-45-0
N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; for 1h; Ambient temperature;

Reference yield:

: 58052-68-9
2,5-diamino-4-methyl-6-thioxo-1,6-dihydopyrimidine

: 90072-45-0
N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / KOH, / methanol / 2 h / Ambient temperature

2: 79 percent / sodium nitrite, aq. HCl / H₂O / 1 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium nitrite; In methanol; water;

Reference yield:

: 100-14-1
4-nitrobenzyl chloride

: 90072-45-0
N(7)-Oxide of 2-Amino-4-(4-nitrobenzyl)thiopyrimido<5,4-d>-1,2,3-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / KOH, / methanol / 2 h / Ambient temperature

2: 79 percent / sodium nitrite, aq. HCl / H₂O / 1 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium nitrite; In methanol; water;