avarol dimethyl ether

Base Information

Chemical Name:avarol dimethyl ether
CAS No.:61187-42-6
Molecular Formula:C₂₃H₃₄O₂
Molecular Weight:342.522
Hs Code.:

Synonyms:avarol dimethyl ether

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Chemical Property of avarol dimethyl ether

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Technology Process of avarol dimethyl ether

There total 12 articles about avarol dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 184485-50-5
(-)-(1R,4aS,8aS)-1β,2β,4aβ-trimethyl-1α-[(2',5'-dimethoxyphenyl)methyl]-5-exo-methylene-(3H)-1,4,4a,5,6,7,8,8a-octahydronaphthalene

: 61187-42-6
avarol dimethyl ether

Guidance literature:: rhodium(III) chloride; In ethanol;
DOI:10.1039/CC9960002717

Reference yield:

: 26742-33-6
(4aS)-1,4aβ-dimethyl-4,4a,7,8-tetrahydronaphthalene-2,5(3H,6H)-dione-5-ethyeneacetal

: 61187-42-6
avarol dimethyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / Li, liq. NH₃

2: 86 percent

3: PPTS / acetone

4: H₂, Et₃N / Pd/C

5: 85 percent

6: 92 percent / RhCl₃ / ethanol

With ammonia; hydrogen; pyridinium p-toluenesulfonate; lithium; triethylamine; palladium on activated charcoal; rhodium(III) chloride; In ethanol; acetone;
DOI:10.1039/CC9960002717

Reference yield:

: 184485-46-9
(1S,4aS)-(+)-trans-1α-[(2,5-dimethoxyphenyl)methyl]-1β,4aβ-dimethyl-5-(2-methyl-1,3-dioxolan-2-yl)-hexahydro-2,5(3H,6H)-naphthalenedione

: 61187-42-6
avarol dimethyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent

2: PPTS / acetone

3: H₂, Et₃N / Pd/C

4: 85 percent

5: 92 percent / RhCl₃ / ethanol

With hydrogen; pyridinium p-toluenesulfonate; triethylamine; palladium on activated charcoal; rhodium(III) chloride; In ethanol; acetone;
DOI:10.1039/CC9960002717