4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

Base Information

Chemical Name:4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate
CAS No.:1345959-48-9
Molecular Formula:CF₃O₃S*C₁₇H₁₉N₂O₄
Molecular Weight:464.419
Hs Code.:

Synonyms:4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

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Chemical Property of 4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

There total 3 articles about 4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1345959-29-6
4-(((1H-imidazole-1-carbonyl)oxy)methyl)-1-methylpyridin-1-ium trifluoromethanesulfonate

: 94-09-7
p-aminoethylbenzoate

: 1345959-48-9
4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

Guidance literature:: In acetonitrile; at 60 ℃;
DOI:10.1021/ol202456d

Reference yield:

: 1345959-27-4
4-(((1H-imidazole-1-carbonyl)oxy)methyl)-1-methylpyridin-1-ium iodide

: 1345959-48-9
4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 1 h

2: acetonitrile / 60 °C

In acetonitrile;
DOI:10.1021/ol202456d

Reference yield:

: 6457-57-4
4-(hydroxymethyl)-1-methylpyridin-1-ium iodide

: 1345959-48-9
4-((4-(ethoxycarbonyl)phenylcarbamoyloxy)methyl)-1-methylpyridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / -30 °C

2: acetonitrile / 1 h

3: acetonitrile / 60 °C

In acetonitrile;
DOI:10.1021/ol202456d