[(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)]

Base Information

Chemical Name:[(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)]
CAS No.:704903-17-3
Molecular Formula:C₃₇H₃₈NNiOP
Molecular Weight:602.379
Hs Code.:

Synonyms:[(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)]

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Chemical Property of [(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)]

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Technology Process of [(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)]

There total 1 articles about [(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 704902-92-1
[(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)chloride)]

: sodium trimethoxyborohydride

: 704903-17-3
[(2-(2,6-diisopropyl)anilinotropone)nickel(triphenylphosphine)(hydride)]

Guidance literature:: In diethyl ether; byproducts: B(OMe)3; charging of Schlenk tube with (PPh3)NiCl(2-(2,6-diisopropyl)anilinotropone) and NaHB(OMe)3 under Ar; cooling in an ice bath; addn. of Et2O; stirring for 4 h; filtration through florisil; removal of solvent in vac.; elem. anal.;
DOI:10.1021/ja030634g