C₉₅H₁₀₅N₅O₈Zn

Base Information

• Chemical Name: C₉₅H₁₀₅N₅O₈Zn
• CAS No.: 1373941-07-1
• Molecular Formula: C₉₅H₁₀₅N₅O₈Zn
• Molecular Weight: 1510.3
• Mol file: 1373941-07-1.mol

Synonyms:C₉₅H₁₀₅N₅O₈Zn

Chemical Property of C₉₅H₁₀₅N₅O₈Zn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₉₅H₁₀₅N₅O₈Zn

There total 2 articles about C₉₅H₁₀₅N₅O₈Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

4-iodobenzoic acid (619-58-9) + C68H84N4O4Zn + N,N-bis(4-methoxyphenyl)-4'-iodophenylamine (201802-15-5) → C95H105N5O8Zn (1373941-07-1)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; triethylamine; In tetrahydrofuran; for 4.5h; Reflux;

Reference yield: 34.0%

4-iodobenzoic acid (619-58-9) + [5,15-di(triisopropylsilyl)ethynyl-10,20-bis(2,6-dioctoxyphenyl)porphinato] zinc(II) (1391758-15-8) + N,N-bis(4-methoxyphenyl)-4'-iodophenylamine (201802-15-5) → C95H105N5O8Zn (1373941-07-1)

Guidance literature:

[5,15-di(triisopropylsilyl)ethynyl-10,20-bis(2,6-dioctoxyphenyl)porphinato] zinc(II); With tetrabutyl ammonium fluoride; at 20 ℃; for 1h;

With water;

4-iodobenzoic acid; N,N-bis(4-methoxyphenyl)-4'-iodophenylamine; Further stages;

DOI:10.1039/c2cc31111a

upstream raw materials:

4-iodobenzoic acid

[5,15-di(triisopropylsilyl)ethynyl-10,20-bis(2,6-dioctoxyphenyl)porphinato] zinc(II)

N,N-bis(4-methoxyphenyl)-4'-iodophenylamine

Refernces

• 1、 Ripolles-Sanchis, Teresa,Guo, Bo-Cheng,Wu, Hui-Ping,Pan, Tsung-Yu,Lee, Hsuan-Wei,Raga, Sonia R.,Fabregat-Santiago, Francisco,Bisquert, Juan,Yeh, Chen-Yu,Diau, Eric Wei-Guang. "Design and characterization of alkoxy-wrapped push-pull porphyrins for dye-sensitized solar cells". supporting information; experimental part. p. 4368 - 4370. Retrieved 2012/06/16.