4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

Base Information

Chemical Name:4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate
CAS No.:304015-18-7
Molecular Formula:C₂₃H₁₉N₃O₁₀
Molecular Weight:497.418
Hs Code.:

Synonyms:4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

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Chemical Property of 4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

Chemical Property:

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Technology Process of 4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

There total 4 articles about 4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 304015-17-6
2-methoxy-4-nitrobenzyl 4-(hydroxymethyl)phenylcarbamate

: 304015-18-7
4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1016/j.bmc.2005.03.055

Reference yield:

: 136507-14-7
(2-methoxy-4-nitrophenyl)methanol

: 304015-18-7
4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / ethyldiisopropylamine / tetrahydrofuran / 16 h / 20 °C

2: 77 percent / triethylamine; 1-hydroxybenzotriazole; molecular sieves 4 Angstroem / tetrahydrofuran / 16 h / 20 °C

3: 95 percent / hydrochloric acid / methanol / 1 h / 20 °C

4: 56 percent / ethyldiisopropylamine / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; 4 A molecular sieve; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2005.03.055

Reference yield:

: 304015-15-4
2-methoxy-4-nitrobenzyl 4-nitrophenyl carbonate

: 304015-18-7
4-({[(2-methoxy-4-nitrobenzyl)oxy]carbonyl}amino)benzyl 4-nitrophenyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / triethylamine; 1-hydroxybenzotriazole; molecular sieves 4 Angstroem / tetrahydrofuran / 16 h / 20 °C

2: 95 percent / hydrochloric acid / methanol / 1 h / 20 °C

3: 56 percent / ethyldiisopropylamine / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; 4 A molecular sieve; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2005.03.055