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Technology Process of (C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

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  • Chemical Name:(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3
  • CAS No.:1337569-83-1
  • Molecular Formula:CF3O3S*C37H31N4P2
  • Molecular Weight:742.698
  • Hs Code.:
(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>

Synonyms:(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

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Chemical Property of (C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3
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Technology Process of (C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

There total 1 articles about (C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C<sub>6</sub>H<sub>4</sub>(NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2
1159579-51-7

C6H4(NC3NH2P(C6H5)2)2

methyl trifluoromethanesulfonate
333-27-7

methyl trifluoromethanesulfonate

(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>
1337569-83-1

(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

Guidance literature:
In dichloromethane; at -78 - 20 ℃; for 2h;
DOI:10.1021/ic201342z

Reference yield: 91.0%

bis(benzonitrile)palladium(II) dichloride
15617-18-2,39958-10-6,14220-64-5

bis(benzonitrile)palladium(II) dichloride

(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>
1337569-83-1

(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>
1337569-86-4

PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

Guidance literature:
In tetrahydrofuran; (Ar, Schlenk) a mixt. of complex and diphosphine was dissolved in THF at-30°C, stirred at room temp. for 3 h; concd. under vac., the residue was washed with diethyl ether, recrystd. from CHCl3 at room temp.;
DOI:10.1021/ic201342z
upstream raw materials:

C6H4(NC3NH2P(C6H5)2)2

methyl trifluoromethanesulfonate

Downstream raw materials:

PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

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