N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

Base Information

Chemical Name:N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine
CAS No.:258337-56-3
Molecular Formula:C₄₈H₅₂N₃O₅P₃
Molecular Weight:843.879
Hs Code.:

N<sup>1</sup>,N<sup>7</sup>-Bis(2',3'-epoxypropyl)-N<sup>1</sup>,N<sup>4</sup>,N<sup>7</sup>-tris(diphenylphosphinoyl)norspermidine

Synonyms:N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

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Technology Process of N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

There total 3 articles about N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 258337-55-2
N¹,N⁴,N⁷-Tris(diphenylphosphinoyl)norspermidine

: 258337-56-3
N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 90 ℃; for 6h;
DOI:10.1039/a903293b

Reference yield:

: 56-18-8
bis(3-aminopropyl)amine

: 258337-56-3
N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NEt₃ / tetrahydrofuran / 1 h

2: 69 percent / NaH / tetrahydrofuran / 6 h / 90 °C

With sodium hydride; triethylamine; In tetrahydrofuran; 1: Phosphinylation / 2: Ring cleavage;
DOI:10.1039/a903293b

Reference yield:

: 1499-21-4
Diphenylphosphinic chloride

: 258337-56-3
N¹,N⁷-Bis(2',3'-epoxypropyl)-N¹,N⁴,N⁷-tris(diphenylphosphinoyl)norspermidine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NEt₃ / tetrahydrofuran / 1 h

2: 69 percent / NaH / tetrahydrofuran / 6 h / 90 °C

With sodium hydride; triethylamine; In tetrahydrofuran; 1: Phosphinylation / 2: Ring cleavage;
DOI:10.1039/a903293b