(E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Base Information

Chemical Name:(E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide
CAS No.:1284229-92-0
Molecular Formula:C₂₀H₂₅N₃O₂S
Molecular Weight:371.503
Hs Code.:

Synonyms:(E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Suppliers and Price of (E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

There total 3 articles about (E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 23117-65-9
2-[(phenylamino)methyl]cyclohexanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1284229-92-0
(E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Guidance literature:: In diethyl ether; at 20 ℃; for 12h;
DOI:10.1002/anie.201006996

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1284229-92-0
(E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: rac-Pro-OH / water; dimethyl sulfoxide / 2.5 h / 46 °C / Microwave irradiation

2: diethyl ether / 12 h / 20 °C

With rac-Pro-OH; In diethyl ether; water; dimethyl sulfoxide; 1: Mannich reaction;
DOI:10.1002/anie.201006996

Reference yield:

: 62-53-3
aniline

: 1284229-92-0
(E)-4-methyl-N'-{2-[(phenylamino)methyl]cyclohexylidene}benzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: rac-Pro-OH / water; dimethyl sulfoxide / 2.5 h / 46 °C / Microwave irradiation

2: diethyl ether / 12 h / 20 °C

With rac-Pro-OH; In diethyl ether; water; dimethyl sulfoxide; 1: Mannich reaction;
DOI:10.1002/anie.201006996