2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

Base Information

Chemical Name:2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid
CAS No.:1206902-68-2
Molecular Formula:C₂₄H₂₃BrO₆
Molecular Weight:487.347
Hs Code.:

Synonyms:2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

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Chemical Property of 2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

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Technology Process of 2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

There total 10 articles about 2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1384190-46-8
2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetaldehyde

: 1206902-68-2
2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; water; tert-butyl alcohol; at 0 ℃; for 1h;
DOI:10.1055/s-0031-1290658

Reference yield:

: 1384190-36-6
2-allyl-4-bromo-6-methoxyphenol 3'-methoxy-4'-benzyloxybenzyl ether

: 1206902-68-2
2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 0 - 20 °C

2: lead(IV) tetraacetate; potassium carbonate / benzene / 3 h / 0 - 20 °C

3: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 0 °C

With sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; lead(IV) tetraacetate; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; acetone; tert-butyl alcohol; benzene;
DOI:10.1055/s-0031-1290658

Reference yield:

: 352019-92-2
2-allyl-4-bromo-6-methoxyphenol

: 1206902-68-2
2-{2-[4-(benzyloxy)-3-methoxybenzyloxy]-5-bromo-3-methoxyphenyl}acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 4 h / 0 - 20 °C

3: lead(IV) tetraacetate; potassium carbonate / benzene / 3 h / 0 - 20 °C

4: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 0 °C

With sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; lead(IV) tetraacetate; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; benzene;
DOI:10.1055/s-0031-1290658