methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

Base Information

Chemical Name:methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate
CAS No.:1207268-90-3
Molecular Formula:C₂₈H₂₆F₃N₃O₄S
Molecular Weight:557.593
Hs Code.:

Synonyms:methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

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Chemical Property of methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

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Technology Process of methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

There total 12 articles about methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207269-29-1
C₁₁H₁₄O₃S

: 1207269-18-8
3-(1'-bromo-benzyl)-4-methyl-1-(4-trifluoromethyl)phenyl-1H-1,2,4-triazole-5(4H)-one

: 1207268-90-3
methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 6h;

Reference yield:

: 103-82-2
phenylacetic acid

: 1207268-90-3
methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 2 h / Reflux

2: water; methanol / 3 h / Reflux

3: trichlorophosphate / toluene / 5 h / 80 - 90 °C

4: dmap / tetrahydrofuran / 12 h / 20 °C

5: dibenzoyl peroxide; N-Bromosuccinimide / chloroform / 12 h / Reflux

6: potassium carbonate / acetonitrile / 6 h / 20 °C

With dmap; N-Bromosuccinimide; sulfuric acid; potassium carbonate; trichlorophosphate; dibenzoyl peroxide; In tetrahydrofuran; methanol; chloroform; water; toluene; acetonitrile;

Reference yield:

: 32281-01-9
4-mercapto-2-methylphenol

: 1207268-90-3
methyl 2-methyl-2-(2-methyl-4-(1-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydro-1H-1,2,4-triazol-3-yl)benzylthio)phenoxy)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: oxygen / ethyl acetate

2: potassium carbonate / acetonitrile / 20 °C

3: hydrogenchloride; zinc / ethanol; water / 0.5 h / 20 °C

4: potassium carbonate / acetonitrile / 6 h / 20 °C

With hydrogenchloride; oxygen; potassium carbonate; zinc; In ethanol; water; ethyl acetate; acetonitrile;