methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate

Base Information

• Chemical Name: methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate
• CAS No.: 129648-83-5
• Molecular Formula: C₂₅H₂₈ClNO₄S
• Molecular Weight: 474.021

Synonyms:methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate

Chemical Property of methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate

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Technology Process of methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate

There total 5 articles about methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 6-isopropyl-2-oxo-2H-cycloheptafuran-3-carboxylate (106021-18-5) → methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate (129648-83-5)

Guidance literature:

Multi-step reaction with 4 steps

1: morpholine

2: AlCl₃, anisole

3: pyridine

4: NaH

With morpholine; pyridine; aluminium trichloride; sodium hydride; methoxybenzene;

DOI:10.1021/jm00171a004

Reference yield:

6-benzyloxy-1-hexanal (101492-91-5) → methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate (129648-83-5)

Guidance literature:

Multi-step reaction with 4 steps

1: morpholine

2: AlCl₃, anisole

3: pyridine

4: NaH

With morpholine; pyridine; aluminium trichloride; sodium hydride; methoxybenzene;

DOI:10.1021/jm00171a004

Reference yield:

methyl 6-isopropyl-3-(4-hydroxybutyl)azulene-1-carboxylate (129648-77-7) → methyl 3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-(1-methyl)ethylazulene-1-carboxylate (129648-83-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: NaH

With pyridine; sodium hydride;

DOI:10.1021/jm00171a004

upstream raw materials:

4-Chlorobenzenesulfonamide

methyl 6-isopropyl-2-oxo-2H-cycloheptafuran-3-carboxylate

6-benzyloxy-1-hexanal

methyl 6-isopropyl-3-(4-hydroxybutyl)azulene-1-carboxylate

Downstream raw materials:

3-<4-(4-chlorobenzenesulfonylamino)butyl>-6-isopropylazulene-1-sulfonate

6-(2-Benzoyloxy-1-hydroxy-1-methyl-ethyl)-3-[4-(4-chloro-benzenesulfonylamino)-butyl]-azulene-1-carboxylic acid methyl ester

N-(4-{6-[2-(tert-Butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-azulen-1-yl}-butyl)-4-chloro-benzenesulfonamide

6-(1-Benzoyloxymethyl-vinyl)-3-[4-(4-chloro-benzenesulfonylamino)-butyl]-azulene-1-carboxylic acid methyl ester

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