3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

Base Information

Chemical Name:3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide
CAS No.:1580507-74-9
Molecular Formula:C₁₁H₂₂NO₂*I
Molecular Weight:327.206
Hs Code.:

Synonyms:3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

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Chemical Property of 3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

Chemical Property:

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Technology Process of 3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

There total 4 articles about 3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 36365-99-8
methyl 3-(dimethylamino)cyclohexanecarboxylate

: 74-88-4
methyl iodide

: 1580507-74-9
3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

Guidance literature:: In methanol; at 20 ℃; for 48h;
DOI:10.1021/jm401603e

Reference yield:

: C₁₀H₁₉NO₂*ClH

: 1580507-74-9
3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane / 7 h / 20 °C

2: methanol / 48 h / 20 °C

With potassium carbonate; In methanol; dichloromethane;
DOI:10.1021/jm401603e

Reference yield:

: 16636-51-4,25912-50-9,34583-99-8,38541-66-1,57043-02-4,81131-39-7,81131-40-0,41235-88-5,933445-51-3,933445-54-6
3-aminocyclohexanecarboxylic acid

: 1580507-74-9
3-(methoxycarbonyl)-N,N,N-trimethylcyclohexanaminium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: formic acid / 25 h / Reflux

2: acetyl chloride / 24 h / 42 °C

3: potassium carbonate / dichloromethane / 7 h / 20 °C

4: methanol / 48 h / 20 °C

With formic acid; potassium carbonate; acetyl chloride; In methanol; dichloromethane;
DOI:10.1021/jm401603e