triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

Base Information

Chemical Name:triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane
CAS No.:1606161-66-3
Molecular Formula:C₃₉H₅₈O₄S₂Si
Molecular Weight:683.105
Hs Code.:

Synonyms:triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

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Technology Process of triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

There total 1 articles about triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 13154-24-0
triisopropylsilyl chloride

: 108713-89-9
(2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentan-1-ol

: 1606161-66-3
triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

Guidance literature:: With dmap; In pyridine; at 20 ℃; for 14h;

Reference yield: 97.0%

: 1606161-66-3
triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

: 1606161-67-4
(2R,3R,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentanal

Guidance literature:: With N-Bromosuccinimide; water; In acetone; at 0 ℃; for 0.5h;

Reference yield:

: 1606161-66-3
triisopropyl-((2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentyloxy)silane

: 1606161-68-5
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: water; N-Bromosuccinimide / acetone / 0.5 h / 0 °C

2: methanol; pyridine / 24 h / 60 °C

3: acetic acid; sodium cyanoborohydride

With N-Bromosuccinimide; water; sodium cyanoborohydride; acetic acid; In pyridine; methanol; acetone;