O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

Base Information

Chemical Name:O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine
CAS No.:1606161-68-5
Molecular Formula:C₄₂H₅₇NO₅Si
Molecular Weight:684.004
Hs Code.:

Synonyms:O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

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Chemical Property of O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

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Technology Process of O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

There total 6 articles about O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 622-33-3
N-benzyloxyamine

: 1606161-67-4
(2R,3R,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentanal

: 1606161-68-5
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

Guidance literature:: N-benzyloxyamine; (2R,3R,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentanal; With pyridine; In methanol; at 60 ℃; for 24h;

With sodium cyanoborohydride; acetic acid; for 0.333333h;

Reference yield:

: C₄₂H₅₅NO₅Si

: 1606161-68-5
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

Guidance literature:: With sodium cyanoborohydride; acetic acid;

Reference yield:

: 108713-89-9
(2R,3R,4R)-2,3,4-tris-benzyloxy-5,5-bis-ethylsulfanyl-pentan-1-ol

: 1606161-68-5
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-pentyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / pyridine / 14 h / 20 °C

2: water; N-Bromosuccinimide / acetone / 0.5 h / 0 °C

3: methanol; pyridine / 24 h / 60 °C

4: acetic acid; sodium cyanoborohydride

With dmap; N-Bromosuccinimide; water; sodium cyanoborohydride; acetic acid; In pyridine; methanol; acetone;