(6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole

Base Information

• Chemical Name: (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole
• CAS No.: 217448-31-2
• Molecular Formula: C₂₆H₂₅N₃
• Molecular Weight: 379.505

Synonyms:(6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole

Chemical Property of (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole

Chemical Property:

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Technology Process of (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole

There total 32 articles about (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C26H28N2O2 (217448-29-8) → (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole (217448-31-2)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 48h; Heating;

DOI:10.1016/S0040-4039(98)01788-2

Reference yield: 81.0%

1-amino-2-butyne hydrochloride (50329-23-2) + (6S,10S)-(-)-9-formyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctaindole (217448-24-3) → (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole (217448-31-2)

Guidance literature:

With montmorillonite K₁₀ Clay; 1,8-diazabicyclo[5.4.0]undec-7-ene; In chlorobenzene; at 150 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.201811812

Reference yield: 48.0%

benzyl bromide (100-39-0) + (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole (93552-58-0) → (6S,13S)-4-ethyl-6,7,12,13-tetrahydro-14-(phenylmethyl)-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole (217448-31-2)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 0.666667h;

DOI:10.1016/j.tet.2007.07.070

upstream raw materials:

C₂₆H₂₈N₂O₂

benzyl bromide

(6S,13S)-4-ethyl-6,7,12,13-tetrahydro-6,13-imino-5H-pyrido[3',4':5,6]cyclooct[1,2-b]indole

(S)-α-(5-oxazolyl)-1H-indole-3-ethanamine

Downstream raw materials:

(-)-N_b-benzylsuaveoline

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