2-Chlor-3ξ--acrylonitril

Base Information

• Chemical Name: 2-Chlor-3ξ--acrylonitril
• CAS No.: 5697-45-0
• Molecular Formula: C₁₀H₈ClNO₂S
• Molecular Weight: 241.698

Synonyms:2-Chlor-3ξ--acrylonitril

Chemical Property of 2-Chlor-3ξ--acrylonitril

Chemical Property:

Purity/Quality:

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Technology Process of 2-Chlor-3ξ--acrylonitril

There total 2 articles about 2-Chlor-3ξ--acrylonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dichloroacrylonitrile (3533-66-2) + sodium 4-methylbenzenesulfinate (824-79-3) → 2-Chlor-3ξ--acrylonitril (5697-45-0)

Guidance literature:

In N,N-dimethyl-formamide;

DOI:10.1016/0040-4020(67)85064-6

Reference yield:

→ 2-Chlor-3ξ--acrylonitril (5697-45-0)

Guidance literature:

2,3-Dichlor-acrylonitril I (cis-trans Gemisch), Na- II, wss. A., 0grad;

Reference yield:

2-Chlor-3ξ--acrylonitril (5697-45-0) + sodium 4-methylbenzenesulfinate (824-79-3) → p-tolylsulfonylmethyl isocyanide (5697-44-9)

Guidance literature:

In ethanol;

DOI:10.1016/0040-4020(67)85064-6

upstream raw materials:

2,3-dichloroacrylonitrile

sodium 4-methylbenzenesulfinate

Downstream raw materials:

p-tolylsulfonylmethyl isocyanide

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