2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

Base Information

Chemical Name:2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile
CAS No.:94833-60-0
Molecular Formula:C₂₄H₁₈Br₂N₂OS
Molecular Weight:542.294
Hs Code.:

Synonyms:2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

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Chemical Property of 2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

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Technology Process of 2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

There total 4 articles about 2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 94640-03-6
4-(4-bromophenyl)-2-thioxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 94833-60-0
2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;

Reference yield: 72.0%

: 670-80-4
4-cyclohexen-1-ylmorpholine

: 125219-60-5
2,6-diamino-4-(4-bromophenyl)-4H-thiopyran-3,5-dicarbonitrile

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 94833-60-0
2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

Guidance literature:: 4-cyclohexen-1-ylmorpholine; 2,6-diamino-4-(4-bromophenyl)-4H-thiopyran-3,5-dicarbonitrile; In ethanol; for 2h; Heating;

para-bromophenacyl bromide; With potassium hydroxide; In ethanol; for 4h; Further stages.;
DOI:10.1134/s1070428008030172

Reference yield:

: 2826-24-6
4-bromobenzylidenemalononitrile

: 94833-60-0
2-(4-bromobenzoylmethylsulfanyl)-4-(4-bromophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / diethylamine / methanol / 168 h / Ambient temperature

2: 89 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / Ambient temperature

With potassium hydroxide; diethylamine; In methanol; N,N-dimethyl-formamide;