chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin

Base Information

Chemical Name:chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin
CAS No.:854589-59-6
Molecular Formula:C₃₆H₃₆ClMnN₄
Molecular Weight:615.1
Hs Code.:

Synonyms:chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin

Suppliers and Price of chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin

There total 1 articles about chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13446-03-2
manganese(II) bromide

: 7647-01-0,15364-23-5
hydrogenchloride

: 10-phenyl-(2,18-diethyl-3,7,8,12,13,17-hexamethyl)porphyrin

: 854589-59-6
chloromanganese-13,17-diethyl-2,3,7,8,12,18-hexamethyl-5-phenylporphyrin

Guidance literature:: With 2,6-lutidine; In tetrahydrofuran; methanol; under Ar, protection from light; solns. of porphyrin in THF and MnBr2 inmethanol mixed, mixt. refluxed in the presence of 2,6-lutidine for 3 h; evapn., chromy. (Al2O3, CH2Cl2/MeOH (92/8), then (9:1)), evapn., dissolved in CH2Cl2, washed with 0.1 M aq. HCl, org. layer dried over MgSO4, evapn., crystn. from CH2Cl2/heptane, washed with heptane and pentane, dried under vac. at 40°C;
DOI:10.1021/ic0501622