[(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

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Chemical Name:[(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester
CAS No.:199006-26-3
Molecular Formula:C₅₄H₅₆N₄O₇S
Molecular Weight:905.127
Hs Code.:

[(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

Synonyms:[(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

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Chemical Property of [(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

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Technology Process of [(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

There total 2 articles about [(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6401-63-4
N-benzyloxycarbonyl-L-leucyl-L-phenylalanine

: (E)-(S)-4-Amino-6-benzenesulfonyl-hex-5-enoic acid trityl-amide

: 199006-26-3
[(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

Guidance literature:: With 4-methyl-morpholine; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 23 ℃; for 18h;
DOI:10.1021/jm980068d

Reference yield:

: {(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allyl}-carbamic acid tert-butyl ester

: 199006-26-3
[(S)-1-((S)-1-{(E)-(S)-3-Benzenesulfonyl-1-[2-(trityl-carbamoyl)-ethyl]-allylcarbamoyl}-2-phenyl-ethylcarbamoyl)-3-methyl-butyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / dioxane / 3 h / 23 °C

2: 1-hydroxybenzotriazole hydrate, 4-methylmorpholine, 1-(3-dimethylamino)propyl-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 18 h / 23 °C

With 4-methyl-morpholine; hydrogenchloride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm980068d