tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane

Base Information

• Chemical Name: tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane
• CAS No.: 235434-16-9
• Molecular Formula: C₃₂H₄₄O₂Si
• Molecular Weight: 488.786

Synonyms:tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane

Chemical Property of tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane

Chemical Property:

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Technology Process of tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane

There total 3 articles about tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol (235434-15-8) + methyl iodide (74-88-4) → tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane (235434-16-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1039/a901392j

Reference yield:

3-[(Z)-2-Iodovinyl]-3-methylcyclohexa-1,4-diene (181576-39-6) → tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane (235434-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / t-BuLi / tetrahydrofuran / -78 °C

2: 96 percent / NaH / dimethylformamide / 0 - 20 °C

With tert.-butyl lithium; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1039/a901392j

Reference yield:

4-(tert-butyldiphenysilanyloxy)-2,2-dimethylbutyraldehyde (187869-61-0) → tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane (235434-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / t-BuLi / tetrahydrofuran / -78 °C

2: 96 percent / NaH / dimethylformamide / 0 - 20 °C

With tert.-butyl lithium; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1039/a901392j

upstream raw materials:

6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

methyl iodide

3-[(Z)-2-Iodovinyl]-3-methylcyclohexa-1,4-diene

4-(tert-butyldiphenysilanyloxy)-2,2-dimethylbutyraldehyde

Downstream raw materials:

(Z)-4-Methoxy-3,3-dimethyl-6-(1-methyl-4-trimethylsilanyl-cyclohexa-2,5-dienyl)-hex-5-en-1-ol

(Z)-4-Methoxy-3,3-dimethyl-6-(1-methyl-4-trimethylsilanyl-cyclohexa-2,5-dienyl)-hex-5-enal

(Z)-4-Methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-en-1-ol

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