C₂₂H₂₇BrO₃

Base Information

Chemical Name:C₂₂H₂₇BrO₃
CAS No.:1322705-96-3
Molecular Formula:C₂₂H₂₇BrO₃
Molecular Weight:419.359
Hs Code.:

C<sub>22</sub>H<sub>27</sub>BrO<sub>3</sub>

Synonyms:C₂₂H₂₇BrO₃

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Chemical Property of C₂₂H₂₇BrO₃

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Technology Process of C₂₂H₂₇BrO₃

There total 7 articles about C₂₂H₂₇BrO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1322705-85-0
C₂₂H₂₈O₃

: 1322705-96-3
C₂₂H₂₇BrO₃

Guidance literature:: With bromine; In chloroform;

Reference yield:

: (R)-2-allyl-2,6,6-trimethylcyclohexanone

: 1322705-96-3
C₂₂H₂₇BrO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxygen / copper(II) acetate monohydrate; palladium dichloride / water; ISOPROPYLAMIDE / 60 h / 22 °C / 760.05 Torr

2.1: potassium hydroxide / xylenes / 11 h / 110 °C / Inert atmosphere

3.1: acetonitrile; acetone / 22.5 h / Irradiation; quartz test tubes

3.2: 0.5 h

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C / Inert atmosphere

5.1: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 7.5 h / 120 °C / Inert atmosphere; microwave

6.1: bromine / chloroform

With tetrabutyl ammonium fluoride; bromine; oxygen; potassium hydroxide; sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; copper(II) acetate monohydrate; palladium dichloride; In tetrahydrofuran; chloroform; ISOPROPYLAMIDE; water; acetone; acetonitrile; xylenes; 1.1: Wacker Oxidation;

Reference yield:

: (R)-2,2,6-trimethyl-6-(2-oxopropyl)cyclohexanone

: 1322705-96-3
C₂₂H₂₇BrO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / xylenes / 11 h / 110 °C / Inert atmosphere

2.1: acetonitrile; acetone / 22.5 h / Irradiation; quartz test tubes

2.2: 0.5 h

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C / Inert atmosphere

4.1: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 7.5 h / 120 °C / Inert atmosphere; microwave

5.1: bromine / chloroform

With tetrabutyl ammonium fluoride; bromine; potassium hydroxide; sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; chloroform; acetone; acetonitrile; xylenes;