methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

Base Information

Chemical Name:methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside
CAS No.:845510-93-2
Molecular Formula:C₅₅H₄₇NO₉
Molecular Weight:865.979
Hs Code.:

Synonyms:methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

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Chemical Property of methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

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Technology Process of methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

There total 4 articles about methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 76-83-5
trityl chloride

: 98-88-4
benzoyl chloride

: 671224-92-3
methyl 2-deoxy-2-(fluoren-9-yl-methoxycarbonylamino)-β-D-glucopyranoside

: 845510-93-2
methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

Guidance literature:: trityl chloride; methyl 2-deoxy-2-(fluoren-9-yl-methoxycarbonylamino)-β-D-glucopyranoside; With pyridine; at 85 ℃; for 2h;

benzoyl chloride; at 20 ℃; for 3.5h;
DOI:10.1016/j.tet.2004.11.024

Reference yield:

: 4710-88-7
3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-glucopyranosyl bromide hydrobromide

: 845510-93-2
methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 76 percent / pyridine / 1 h

2.1: 95 percent / acetyl chloride; MeOH / 24 h / 20 °C

3.1: 76 percent / NaHCO₃ / H₂O; acetone / 15 h

4.1: pyridine / 2 h / 85 °C

4.2: 63 percent / 3.5 h / 20 °C

With pyridine; methanol; sodium hydrogencarbonate; acetyl chloride; In water; acetone;
DOI:10.1016/j.tet.2004.11.024

Reference yield:

: 3867-93-4
methyl 2-amino-2-deoxy-β-D-glucopyranoside hydrochloride

: 845510-93-2
methyl 3,4-di-O-benzoyl-2-(9-fluorenylmethoxycarbonylamino)-2-deoxy-6-O-triphenylmethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / NaHCO₃ / H₂O; acetone / 15 h

2.1: pyridine / 2 h / 85 °C

2.2: 63 percent / 3.5 h / 20 °C

With pyridine; sodium hydrogencarbonate; In water; acetone;
DOI:10.1016/j.tet.2004.11.024