benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

Base Information

Chemical Name:benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)
CAS No.:1287794-79-9
Molecular Formula:C₁₅H₁₀F₃IN₂O₃
Molecular Weight:450.156
Hs Code.:

Synonyms:benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

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Chemical Property of benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

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Technology Process of benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

There total 3 articles about benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 29632-74-4
2-fluro-4-iodoaniline

: 1287794-78-8
benzene, 1,2,3-trifluoro-4-nitro-5-(2-propen-1-yloxy)

: 1287794-79-9
benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

Guidance literature:: 2-fluro-4-iodoaniline; With lithium hexamethyldisilazane; In tetrahydrofuran; for 0.5h;

benzene, 1,2,3-trifluoro-4-nitro-5-(2-propen-1-yloxy); In tetrahydrofuran; at -78 ℃; for 4h;
DOI:10.1016/j.bmc.2016.12.014

Reference yield:

: 99627-05-1
3,4,5-trifluorophenol

: 1287794-79-9
benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid; acetic acid / 0.75 h / 4 - 20 °C

2.1: potassium carbonate / acetone / 2 h / Reflux

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

3.2: 17 h / -78 - 20 °C

With nitric acid; potassium carbonate; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; acetone;

Reference yield:

: 923033-24-3
phenol, 3,4,5-trifluoro-2-nitro

: 1287794-79-9
benzenamine, 2,3-difluoro-N-(2-fluoro-4-iodophenyl)-6-nitro-5-(2-propen-1-yloxy)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 2 h / Reflux

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.2: 17 h / -78 - 20 °C

With potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; acetone;