2-acetylbenzyl acetate

Base Information

• Chemical Name: 2-acetylbenzyl acetate
• CAS No.: 99865-30-2
• Molecular Formula: C₁₁H₁₂O₃
• Molecular Weight: 192.214
• Mol file: 99865-30-2.mol

Synonyms:2-acetylbenzyl acetate

Chemical Property of 2-acetylbenzyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-acetylbenzyl acetate

There total 2 articles about 2-acetylbenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

trimethylsiloxyethene (6213-94-1) + (2-iodophenyl)methyl acetate (80953-51-1) → 2-acetylbenzyl acetate (99865-30-2)

Guidance literature:

With palladium diacetate; triethylamine; triphenylphosphine; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 20 - 100 ℃; for 2h; Reagent/catalyst; Solvent; Temperature; regioselective reaction; Microwave irradiation;

DOI:10.1002/adsc.201200334

Reference yield:

acetic acid-(2-ethyl-benzyl ester) (100058-58-0) → 2-acetylbenzyl acetate (99865-30-2)

Guidance literature:

With chromium(VI) oxide; acetic acid;

Reference yield:

2-acetylbenzyl acetate (99865-30-2) → 2-(Hydroxymethyl)acetophenon (32521-21-4)

Guidance literature:

With potassium hydroxide;

upstream raw materials:

acetic acid-(2-ethyl-benzyl ester)

trimethylsiloxyethene

(2-iodophenyl)methyl acetate

Downstream raw materials:

2-(Hydroxymethyl)acetophenon