3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

Base Information

Chemical Name:3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester
CAS No.:102696-81-1
Molecular Formula:C₁₄H₁₅ClO₄
Molecular Weight:282.724
Hs Code.:

Synonyms:3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

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Chemical Property of 3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

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Technology Process of 3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

There total 1 articles about 3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49827-44-3
dimethyl 2,2-dimethylsuccinate

: 587-04-2
m-Chlorobenzaldehyde

: 102696-81-1
3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

Guidance literature:: With sodium hydride; In benzene; Yield given;
DOI:10.1021/je00045a033

Reference yield: 93.0%

: 102696-81-1
3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

: 102696-88-8
3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid

Guidance literature:: With potassium hydroxide; In methanol; water; for 4h; Heating;
DOI:10.1021/je00045a033

Reference yield:

: 102696-81-1
3-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-2,2-dimethyl-succinic acid 4-methyl ester

: 102696-95-7
4-[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-3,3-dimethyl-dihydro-furan-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / potassium hydroxide / H₂O; methanol / 4 h / Heating

2: 92 percent / acetic anhydride / 5 h / Heating

With potassium hydroxide; acetic anhydride; In methanol; water;
DOI:10.1021/je00045a033