N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

Base Information

Chemical Name:N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine
CAS No.:289491-94-7
Molecular Formula:C₂₃H₂₇N₃O₄S
Molecular Weight:441.551
Hs Code.:

N<sup>α</sup>-[N<sup>2</sup>-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

Synonyms:N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

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Chemical Property of N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

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Technology Process of N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

There total 3 articles about N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 81225-90-3
(S)-2-(2-Amino-ethylamino)-3-phenyl-propionic acid

: 289491-94-7
N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

Guidance literature:: With lithium carbonate; In water; acetonitrile; at 0 ℃; for 4h;
DOI:10.1016/S0040-4039(00)00444-5

Reference yield:

: 166108-59-4
N^α-[N²-(tert-butoxycarbonyl)aminoethyl]-L-phenylalanine

: 289491-94-7
N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: anisole; AlCl₃ / CH₂Cl₂; nitromethane / 0.25 h / 20 °C

2: aq. Li₂CO₃ / acetonitrile / 4 h / 0 °C

With aluminium trichloride; lithium carbonate; methoxybenzene; In nitromethane; dichloromethane; acetonitrile;
DOI:10.1002/chem.200305448

Reference yield:

: 962-39-0
L-Phenylalanine benzyl ester

: 289491-94-7
N^α-[N²-(5-dimethylamino-1-naphthalenesulfonyl)aminoethyl]-L-phenylalanine

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₃CN; CH₃COOH / methanol / 2 h / 20 °C

2: anisole; AlCl₃ / CH₂Cl₂; nitromethane / 0.25 h / 20 °C

3: aq. Li₂CO₃ / acetonitrile / 4 h / 0 °C

With aluminium trichloride; lithium carbonate; sodium cyanoborohydride; acetic acid; methoxybenzene; In methanol; nitromethane; dichloromethane; acetonitrile;
DOI:10.1002/chem.200305448