Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

Base Information

Chemical Name:Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester
CAS No.:208586-34-9
Molecular Formula:C₂₅H₃₃NO₄S
Molecular Weight:443.607
Hs Code.:

Synonyms:Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

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Chemical Property of Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

Chemical Property:

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Technology Process of Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

There total 6 articles about Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 208586-34-9
Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / K₂CO₃ / dioxane; H₂O

2: 1.) diisopropylazodicarboxylate, Ph₃P / 1.) THF, 1 h, 2.) THF, overnight

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In 1,4-dioxane; water;
DOI:10.1021/ja973464e

Reference yield:

: 14593-43-2
benzyl allyl ether

: 208586-34-9
Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / benzene / 25 h / Heating

2: 72 percent / NiCl₂, LiAlH₄ / tetrahydrofuran / 10 h / Ambient temperature

3: 99 percent / K₂CO₃ / dioxane; H₂O

4: 1.) diisopropylazodicarboxylate, Ph₃P / 1.) THF, 1 h, 2.) THF, overnight

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; nickel dichloride; In tetrahydrofuran; 1,4-dioxane; water; benzene;
DOI:10.1021/ja973464e

Reference yield:

: 74635-18-0
N-benzylmethylene nitrone

: 208586-34-9
Thioacetic acid S-[3-(benzyl-tert-butoxycarbonyl-amino)-1-benzyloxymethyl-propyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / benzene / 25 h / Heating

2: 72 percent / NiCl₂, LiAlH₄ / tetrahydrofuran / 10 h / Ambient temperature

3: 99 percent / K₂CO₃ / dioxane; H₂O

4: 1.) diisopropylazodicarboxylate, Ph₃P / 1.) THF, 1 h, 2.) THF, overnight

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; nickel dichloride; In tetrahydrofuran; 1,4-dioxane; water; benzene;
DOI:10.1021/ja973464e