C₂₉H₄₆O₅SSi

Base Information

Chemical Name:C₂₉H₄₆O₅SSi
CAS No.:1403235-22-2
Molecular Formula:C₂₉H₄₆O₅SSi
Molecular Weight:534.833
Hs Code.:

C<sub>29</sub>H<sub>46</sub>O<sub>5</sub>SSi

Synonyms:C₂₉H₄₆O₅SSi

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Chemical Property of C₂₉H₄₆O₅SSi

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Technology Process of C₂₉H₄₆O₅SSi

There total 6 articles about C₂₉H₄₆O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1403235-21-1
C₂₂H₄₀O₃Si

: 98-59-9
p-toluenesulfonyl chloride

: 1403235-22-2
C₂₉H₄₆O₅SSi

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol302309c

Reference yield:

: 1403235-36-8
C₁₄H₂₀O

: 1403235-22-2
C₂₉H₄₆O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tert-butyl alcohol; water; tetrahydrofuran / 12 h / Inert atmosphere

1.2: 3 h / 0 - 20 °C / Inert atmosphere

2.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

2.3: 6 h / -78 - 0 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.1: sodium tetrahydroborate / water; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; osmium(VIII) oxide; di-n-butylboryl trifluoromethanesulfonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 2.1: |Evans Aldol Reaction / 2.2: |Evans Aldol Reaction / 2.3: |Evans Aldol Reaction;
DOI:10.1021/ol302309c

Reference yield:

: 82538-49-6
(3S)-5-(benzyloxy)-3-methylpentanal

: 1403235-22-2
C₂₉H₄₆O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

1.3: 6 h / -78 - 0 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium tetrahydroborate / water; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; di-n-butylboryl trifluoromethanesulfonate; triethylamine; In tetrahydrofuran; dichloromethane; water; 1.1: |Evans Aldol Reaction / 1.2: |Evans Aldol Reaction / 1.3: |Evans Aldol Reaction;
DOI:10.1021/ol302309c