(S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

Base Information

Chemical Name:(S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate
CAS No.:1415037-67-0
Molecular Formula:C₂₁H₂₄N₄O₇S
Molecular Weight:476.51
Hs Code.:

Synonyms:(S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

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Technology Process of (S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

There total 11 articles about (S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415037-53-4
(R)-1-((tert-butyldiphenylsilyl)oxy)-3-(4-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)butoxy)-propan-2-yl 4-((tert-butyldiphenylsilyl)oxy)benzoate

: 1415037-67-0
(S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c2cc36604e DOI:10.1039/c2cc36604e

Reference yield:

: 1415037-55-6
(S)-3-(4-(4-methoxybenzyloxy)butoxy)propan-1,2-diol

: 1415037-67-0
(S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 - 20 °C / pH 7

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 0 - 20 °C

6: pyridine; / tetrahydrofuran / 20 °C

With pyridine; 1H-imidazole; di-isopropyl azodicarboxylate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: |Mitsunobu Displacement / 4: |Mitsunobu Displacement;
DOI:10.1039/c2cc36604e DOI:10.1039/c2cc36604e

Reference yield:

: 1415037-56-7
(S)-1-(4-methoxyphenyl)-13,13-dimethyl-12,12-diphenyl-2,7,11-trioxa-12-silatetradecan-9-ol

: 1415037-67-0
(S)-1-hydroxy-3-(4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)butoxy)propan-2-yl 4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 - 20 °C / pH 7

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 0 - 20 °C

5: pyridine; / tetrahydrofuran / 20 °C

With pyridine; di-isopropyl azodicarboxylate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; 1: |Mitsunobu Displacement / 3: |Mitsunobu Displacement;
DOI:10.1039/c2cc36604e DOI:10.1039/c2cc36604e