17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione

Base Information

• Chemical Name: 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione
• CAS No.: 129435-33-2
• Molecular Formula: C₂₇H₂₉N₃O₆S
• Molecular Weight: 523.61

Synonyms:17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione

Chemical Property of 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione

There total 2 articles about 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

N-Tosyliminodiacetic acid dichloroanhydride (42031-77-6) + 2,2′-(butane-1,4-diylbis(oxy))dianiline (77804-76-3) → 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.08,13]pentacosa-1(25),8(13),9,11,21,23-hexaene-15,19-dione (129435-33-2)

Guidance literature:

With pyridine; In benzene;

DOI:10.1007/BF00487439

Reference yield:

1,6-bis(2-nitrophenyl)-1,6-dioxahexane (14467-64-2) → 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.08,13]pentacosa-1(25),8(13),9,11,21,23-hexaene-15,19-dione (129435-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / NaBH₄ / 10percent Pd/C / methanol / 0.33 h

2: 25 percent / pyridine / benzene

With pyridine; sodium tetrahydroborate; palladium on activated charcoal; In methanol; benzene;

DOI:10.1007/BF00487439

Reference yield: 78.0%

17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.08,13]pentacosa-1(25),8(13),9,11,21,23-hexaene-15,19-dione (129435-33-2) → 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.08,13]pentacosa-1(25),8(13),9,11,21,23-hexaene (129435-36-5)

Guidance literature:

With sodium tetrahydroborate; In 1,2-dimethoxyethane;

DOI:10.1007/BF00487439

upstream raw materials:

N-Tosyliminodiacetic acid dichloroanhydride

2,2′-(butane-1,4-diylbis(oxy))dianiline

1,6-bis(2-nitrophenyl)-1,6-dioxahexane

Downstream raw materials:

17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 129435-33-2 17-(Toluene-4-sulfonyl)-2,7-dioxa-14,17,20-triaza-tricyclo[19.4.0.0^8,13]pentacosa-1⁽²⁵⁾,8⁽¹³⁾,9,11,21,23-hexaene-15,19-dione

Send

Send

Metric Ton KG G Pound L ML

Send

Send