HC₂(C₆H₄)(C₉H₄O)(O)OMe

Base Information

• Chemical Name: HC₂(C₆H₄)(C₉H₄O)(O)OMe
• CAS No.: 1007391-75-4
• Molecular Formula: C₁₈H₁₂O₃
• Molecular Weight: 276.291
• Mol file: 1007391-75-4.mol

Synonyms:HC₂(C₆H₄)(C₉H₄O)(O)OMe

Chemical Property of HC₂(C₆H₄)(C₉H₄O)(O)OMe

Chemical Property:

Purity/Quality:

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Technology Process of HC₂(C₆H₄)(C₉H₄O)(O)OMe

There total 1 articles about HC₂(C₆H₄)(C₉H₄O)(O)OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-(4-ethynylphenyl)-3-hydroxy-4H-chromen-4-one + methyl iodide (74-88-4) → HC2(C6H4)(C9H4O)(O)OMe (1007391-75-4)

Guidance literature:

With potassium carbonate; In acetonitrile; at 40 ℃;

DOI:10.1016/j.jorganchem.2007.10.046

Reference yield:

HC2(C6H4)(C9H4O)(O)OMe (1007391-75-4) + [RuCl(dppe)2]OTf (253687-41-1) → trans-[RuCl(1,2-bis(diphenylphosphino)ethane)2(C=CH-p-phenyl-(COC6H4C(O)C(OCH3)))](trifluoromethanesulfonate)

Guidance literature:

In dichloromethane; Ru complex was added to soln. of ligand (1 equiv.) in CH2Cl2 under Ar inSchlenk tube; stirred at room temp. overnight; evapd. (vac.);

DOI:10.1016/j.jorganchem.2007.10.046

upstream raw materials:

methyl iodide