ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside
CAS No.:1357153-83-3
Molecular Formula:C₂₈H₃₈O₇S
Molecular Weight:518.672
Hs Code.:

Synonyms:ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

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Technology Process of ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: (2'R,3'R)-ethyl 2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

: 1357153-83-3
ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

Guidance literature:: (2'R,3'R)-ethyl 2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm201571p

Reference yield: 99.0%

: 1357153-83-3
ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

: 1357153-84-4
ethyl 4,6-di-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: With acetic acid; In water; for 1h; Inert atmosphere; Reflux;
DOI:10.1021/jm201571p

Reference yield:

: 1357153-83-3
ethyl (2'R,3'R)-4,6-di-O-benzyl-2,3-di-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-β-D-glucopyranoside

: 212199-12-7
ethyl 2,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / water / 1 h / Inert atmosphere; Reflux

2: tetrabutylammomium bromide; di(n-butyl)tin oxide / acetonitrile / 24 h / Inert atmosphere; Reflux; Molecular sieve

With tetrabutylammomium bromide; di(n-butyl)tin oxide; acetic acid; In water; acetonitrile;
DOI:10.1021/jm201571p