(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

Base Information

Chemical Name:(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate
CAS No.:128501-75-7
Molecular Formula:C₂₁H₂₂N₄O₃S
Molecular Weight:410.497
Hs Code.:

(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<d><1,2,3>triazol-4-one oxime p-toluenesulfonate

Synonyms:(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

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Technology Process of (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

There total 2 articles about (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 103869-96-1
(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

: 98-59-9
p-toluenesulfonyl chloride

: 128501-75-7
(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

Guidance literature:: With sodium hydroxide; In acetone; at 0 ℃; for 0.5h;

Reference yield:

: 97507-59-0
4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

: 128501-75-7
(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / NH₂OH*HCl, NaOAc / H₂O; ethanol / 3 h / Heating

2: 87 percent / 8percent NaOH / acetone / 0.5 h / 0 °C

With sodium hydroxide; hydroxylamine hydrochloride; sodium acetate; In ethanol; water; acetone;